气相色谱法直接测定水中微量有机胺

用配有氢火焰离子化检测器（FID）的气相色谱仪直接测定水中多种微量有机胺。试样经过滤后直接进样，在气相色谱仪上使用CP7448毛细管柱，用外标法测定水中微量甲胺、二甲胺、一乙胺、二乙胺的含量。在所选择的色谱操作条件下，甲胺、二甲胺、一乙胺、二乙胺的质量浓度分别在一定范围内与峰面积呈良好的线性关系。4种组分的回收率分别为96.7％，99．0％，101．2％，99．2％；精密度分别为4．3％，3．7％，5．5％，3．1％；检出限分别为2．0,2．0，1．5，1．5mg/L。该方法操作简便，回收率、精密度高。     

Mechanical Properties with the Functional Group of Additives for Starch/PVA Blend Film

This paper deals with the mechanical properties and degree of swelling (DS) of starch/PVA blend film with the functional groups i.e., hydroxyl and carboxyl group, of additives. Starch/PVA blend films were prepared by using the mixing process. Glycerol (GL) with 3 hydroxyl group, sorbitol (SO) with 6 hydroxyl group, succinic acid (SA) with 2 carboxyl group, malic acid (MA) with 1 hydroxyl and 2 carboxyl group, tartaric acid (TA) with 2 hydroxyl and 2 carboxyl group and citric acid (CA) with 1 hydroxyl and 3 carboxyl group were used as additives. The results of measured tensile strength (TS) and elongation (%E) verified that both hydroxyl and carboxyl group as a functional groups increased the flexibility and strength of the film. Values of DS for GL-added and SA-added films were low. However, DS values of the films added MA, TA or CA with both hydroxyl and carboxyl group were comparatively high. When the film was dried at low temperature, the properties of the films were evidently improved. The reason is probably because the hydrogen bonding was activated at low temperature.     

布袋式除尘器在电厂输煤系统上的应用

针对胜利电厂皮带输煤系统粉尘浓度高、污染环境、影响职工身体健康的问题，用布袋式除尘器替代原有的静电除尘器，并对布袋除尘器辅助系统进行了多处改进和完善，提高了运行的可靠性。投运后粉尘质量浓度由原来的18．3mg／m^3降低至1．68mg／m^3，除尘效率达到了98％以上。     

地铁火灾场景设计探讨

近年来，地铁火灾是火灾科学界研究的热点。火灾场景设计是开展地铁火灾研究的基础环节，它对地铁内的烟气运动和人员疏散有重要的影响。通过对国内外文献的调研发现，地铁火灾场景的设计并无统一明确的表述。在综合前人研究的基础上，对地铁火灾场景中需要确定的火灾荷载和起火点位置进行了初步探讨，并给出了分析结果。     

粘弹性阻尼减震结构研究与应用的新进展

系统总结了国内外粘弹性阻尼器及粘弹性阻尼减震结构研究与应用的进展情况。阐述了粘弹性阻尼材料和粘弹性阻尼器的耗能原理;对目前开发和研究的一些新型粘弹性阻尼器及其性能进行了介绍,同时概述了对保证结构安全性具有重大意义的粘弹性阻尼器的耐久性和耐火性问题,介绍了不同的粘弹性阻尼器计算模型;从结构试验的角度说明了粘弹性阻尼减震结构的特性,着重说明了粘弹性阻尼减震结构的分析方法和设计方法,列举了粘弹性阻尼器的工程应用实例。进而提出了今后粘弹性阻尼器应用于土木工程领域里应加强研究的一些问题。     

淮河流域旱涝易发区农田的陆气相互作用——CO2通量、能量交换和水汽输送的季节变化特征

利用淮河流域旱涝易发区的安徽省寿县农田下垫面陆气相互作用观测试验资料,重点分析观测期内CO2通量、能量交换和水汽输送的季节变化,并讨论了与此有关的辐射分量通量、下垫面反射率、波恩比、能量闭合守恒、土壤温度和土壤湿度的季节变化.结果表明CO2通量、能量分配受地表农作物长势影响明显,其中,水稻灌浆、成熟期,被稻田吸收的CO2通量最大可超过2 mg·m-2·s-1,潜热通量达到正的极大值.稻田光合作用最旺盛时期吸收的CO2通量和释放的潜热通量均大于小麦田光合作用最旺盛时期的对应量.较大土壤热通量对应于较低的土壤水含量.试验观测期的下垫面平均反射率为0.14.作物生长期,稻田表面潜热是下垫面吸收能量的主要消费者,小麦田表面潜热和感热相当.能量闭合率ε的变化范围为0.4～1.     

城市学校建筑抗震防灾安全综合评价

学校的防灾安全越来越得到人们的重视,是城市防灾安全规划中的一项重要内容.在城市化快速发展的时代,新的灾种不断发生,出现自然灾害和人为技术事故的可能性也在增加.     

Measurements of PCB Fluxes into the Atmosphere from a Site Receiving Stabilized Dredged Material

A 50 ha known contaminated site in Bayonne, New Jersey, U.S.A. is permitted to receive up to 3 × 10⁶ m³ of sediment dredged from navigation channels in the New York/New Jersey Harbor. Much of the sediment is expected to contain low to moderate concentrations of industrial and agricultural chemicals, including Polychlorinated Biphenyls (PCBs). The dredged material brought to the site is stabilized with cement and then placed as a capping and grading layer. The flux of PCBs from drying stabilized dredged material has been estimated from measurements of PCB air concentrations at two heights above the ground along with micrometeorological observations. A statistically significant gradient in PCB concentrations has been consistently measured in the first 3 m above the ground. Observed PCB fluxes were highest over freshly placed stabilized dredged sediment and decreased as it cured. The highest flux observed in this study was 7214 ng/m²/h, but during subsequent sampling intervals at the same site, the flux estimates decreased by an order of magnitude over a 5-day interval.     

基于CAN总线的分布式安全报警系统

CAN总线是一种多主站局部网络 ,支持分布式控制系统或实时控制系统的通信功能 ,具有检错功能强 ,抗干扰 ,传输速率高等优点 ,广泛应用于工业控制领域。笔者以CAN总线技术为基础 ,用单片机和个人计算机组成分布式安全报警系统 ,该系统具有开放性、全分散体系结构、安装维护简单等特点。笔者介绍了该系统的总体构成及其软件和硬件设计。试验结果表明 ,该系统实现了事故现场、住户与住宅小区三者联系的安全报警功能。系统稳定性好 ,实时性强 ,报警准确。     

国家安全生产监督管理总局部署开展劳防用品专项检查

国家安全生产监督管理总局和全国总工会为深入贯彻《安全生产法》，进一步加强对劳动防护用品的监督管理，确保从业人员的职业安全与健康，最近联合下发通知。要求各地区对生产经营单位劳防用品的配备、管理、使用情况，进行一次全国范围的专项监督检查。